Synthesis, characterization, and crystal structure of bis[4-(3?-benzoyl)thiocarbamidophenyl]ether

dc.authoridARSLAN, N. Burcu/0000-0002-1880-1047
dc.contributor.authorAydin, F.
dc.contributor.authorAykac, D.
dc.contributor.authorArslan, N. Burcu
dc.contributor.authorKazak, C.
dc.date.accessioned2025-01-27T20:45:45Z
dc.date.available2025-01-27T20:45:45Z
dc.date.issued2014
dc.departmentÇanakkale Onsekiz Mart Üniversitesi
dc.description.abstractThe title compound, bis[4-(3'-benzoyl)thiocarbamidophenyl]ether, was synthesized by the reaction of benzoylisothiocyanate with 4,4'-diaminodiphenylether in aprotic solvent. The structure was determinated by means of elemental analysis and FT-IR, H-1-NMR, (1)3C-NMR and MS spectroscopic techniques. The crystal structure was characterized by X-ray syngle crystal analysis: orthorhombic, sp. gr. Pnna, Z = 4. In crystal packing, there are intramolecular hydrogen bond N-Ha <-O generating S(6) motif, and intermolecular hydrogen bond N-Ha <-S forming R (2) (2) (8) ring.
dc.description.sponsorshipCanakkale Onsekiz Mart University [BAP 2008/35]
dc.description.sponsorshipThis work was supported by Canakkale Onsekiz Mart University Research Fund Project BAP 2008/35.
dc.identifier.doi10.1134/S1063774514070050
dc.identifier.endpage960
dc.identifier.issn1063-7745
dc.identifier.issn1562-689X
dc.identifier.issue7
dc.identifier.scopus2-s2.0-84913529894
dc.identifier.scopusqualityQ4
dc.identifier.startpage955
dc.identifier.urihttps://doi.org/10.1134/S1063774514070050
dc.identifier.urihttps://hdl.handle.net/20.500.12428/24704
dc.identifier.volume59
dc.identifier.wosWOS:000345382900005
dc.identifier.wosqualityQ4
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherPleiades Publishing Inc
dc.relation.ispartofCrystallography Reports
dc.relation.publicationcategoryinfo:eu-repo/semantics/openAccess
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.snmzKA_WoS_20250125
dc.subjectMolecular-Structures
dc.subjectNi-Ii
dc.subjectComplexes
dc.subjectThiourea
dc.subjectGeneration
dc.subjectPt(Ii)
dc.subjectNi(Ii)
dc.titleSynthesis, characterization, and crystal structure of bis[4-(3?-benzoyl)thiocarbamidophenyl]ether
dc.typeArticle

Dosyalar