Synthesis, characterization, and crystal structure of bis[4-(3?-benzoyl)thiocarbamidophenyl]ether
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Tarih
2014
Yazarlar
Dergi Başlığı
Dergi ISSN
Cilt Başlığı
Yayıncı
Pleiades Publishing Inc
Erişim Hakkı
info:eu-repo/semantics/closedAccess
Özet
The title compound, bis[4-(3'-benzoyl)thiocarbamidophenyl]ether, was synthesized by the reaction of benzoylisothiocyanate with 4,4'-diaminodiphenylether in aprotic solvent. The structure was determinated by means of elemental analysis and FT-IR, H-1-NMR, (1)3C-NMR and MS spectroscopic techniques. The crystal structure was characterized by X-ray syngle crystal analysis: orthorhombic, sp. gr. Pnna, Z = 4. In crystal packing, there are intramolecular hydrogen bond N-Ha <-O generating S(6) motif, and intermolecular hydrogen bond N-Ha <-S forming R (2) (2) (8) ring.
Açıklama
Anahtar Kelimeler
Molecular-Structures, Ni-Ii, Complexes, Thiourea, Generation, Pt(Ii), Ni(Ii)
Kaynak
Crystallography Reports
WoS Q Değeri
Q4
Scopus Q Değeri
Q4
Cilt
59
Sayı
7
