Synthesis, characterization and thermal degradation kinetics of poly(imino isophthaloyl imino (2,4,8,10-tetraoksoaspiro [5,5] undekan-3,9-dipropylene))

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dc.authoridKaya, İsmet / 0000-0002-9813-2962
dc.authoridDoğan, Fatih / 0000-0002-3088-886X
dc.contributor.authorDoğan, Fatih
dc.contributor.authorAkat, Hakan
dc.contributor.authorKaya, İsmet
dc.date.accessioned2025-01-27T20:14:31Z
dc.date.available2025-01-27T20:14:31Z
dc.date.issued2008
dc.departmentÇanakkale Onsekiz Mart Üniversitesi
dc.description.abstractA new polymer, poly(imino isophthaloyl imino (2,4,8,10-tetraoksoaspiro [5,5] undekan-3,9-dipropylene)) [poly(IPIT)] was synthesized by an interfacial polycondensation reaction. The characterization of poly( IPIT) was conducted by using FT-IR, C-13-NMR, TG and DTA techniques. The kinetics of the thermal degradation of poly( IPIT) was investigated by thermogravimetric analysis at different heating rates. TG curves showed that the thermal decomposition of poly( IPIT) occurred in three stages. The apparent activation energies of thermal decomposition for poly( IPIT), as determined by the Tang method (TM), the Flynn-Wall-Ozawa method (FWO) and the Kissinger-Akahira-Sunose method (KAS) are 58.09, 57.7 and 61.0 kJ/mol for the first stage decomposition, 106.1, 105.6 and 109.8 kJ/mol for the second stage decomposition, and 138.1, 137.5 and 141.4 kJ/mol for the third stage decomposition, respectively.
dc.identifier.doi10.1142/S0256767908002650
dc.identifier.endpage53
dc.identifier.issn0256-7679
dc.identifier.issue1
dc.identifier.scopus2-s2.0-43949109608
dc.identifier.scopusqualityQ1
dc.identifier.startpage47
dc.identifier.urihttps://doi.org/10.1142/S0256767908002650
dc.identifier.urihttps://hdl.handle.net/20.500.12428/21118
dc.identifier.volume26
dc.identifier.wosWOS:000255010500006
dc.identifier.wosqualityQ3
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherWorld Scientific Publ Co Pte Ltd
dc.relation.ispartofChinese Journal of Polymer Science
dc.relation.publicationcategoryinfo:eu-repo/semantics/openAccess
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.snmzKA_WoS_20250125
dc.subjectthermal degradation
dc.subjectkinetic method
dc.subjectpolyamide
dc.titleSynthesis, characterization and thermal degradation kinetics of poly(imino isophthaloyl imino (2,4,8,10-tetraoksoaspiro [5,5] undekan-3,9-dipropylene))
dc.typeArticle

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