Spectroscopic studies and crystal structure of 3-[(2-morpholinoethylimino)methyl]benzene-1,2-diol

Basit Öğe Kaydı
dc.authoridUnver, Huseyin/0000-0003-3968-4385
dc.contributor.authorUenver, Hueseyin
dc.contributor.authorYıldız, Mustafa
dc.contributor.authorOcak, Nazan
dc.contributor.authorDurlu, Tahsin Nuri
dc.date.accessioned2025-01-27T20:56:23Z
dc.date.available2025-01-27T20:56:23Z
dc.date.issued2008
dc.departmentÇanakkale Onsekiz Mart Üniversitesi
dc.description.abstractSchiff base 3-[(2-morpholinoethylimino)methyl]benzene-1,2-diol has been synthesized from the reaction of 4-(2-aminoethyl)morpholine with 2,3-dihydroxybenzaldehyde. The title compound has been characterized by elemental analysis, IR, H-1-NMR, C-13-NMR and UV-visible techniques. The structure of the compound also has been examined crystallographically. For the compound exist as dominant form of enol-imines in both the solutions and solid state. The crystal structure has been solved by direct methods and refined by full-matrix least squares. The title compound crystallize in the monoclinic space group P2(1)/n with a = 12.085(1), b = 8.256(1), c = 13.650(1) angstrom, beta = 108.56(1)degrees, V = 1291.1(2) angstrom(3), D (x) = 1.288 g cm(-3), respectively (R-1 = 0.0336 and wR(2) = 0.0922 for 2117 reflections [I > 2 sigma(1)].
dc.identifier.doi10.1007/s10870-007-9270-1
dc.identifier.endpage108
dc.identifier.issn1074-1542
dc.identifier.issn1572-8854
dc.identifier.issue2
dc.identifier.scopus2-s2.0-38349027095
dc.identifier.scopusqualityQ3
dc.identifier.startpage103
dc.identifier.urihttps://doi.org/10.1007/s10870-007-9270-1
dc.identifier.urihttps://hdl.handle.net/20.500.12428/26389
dc.identifier.volume38
dc.identifier.wosWOS:000252388200005
dc.identifier.wosqualityQ4
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherSpringer/Plenum Publishers
dc.relation.ispartofJournal of Chemical Crystallography
dc.relation.publicationcategoryinfo:eu-repo/semantics/openAccess
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.snmzKA_WoS_20250125
dc.subjectSchiff base
dc.subjectspectroscopy
dc.subjectcrystal structure
dc.subjectFT-IR
dc.subjectH-1-NMR
dc.titleSpectroscopic studies and crystal structure of 3-[(2-morpholinoethylimino)methyl]benzene-1,2-diol
dc.typeArticle

Dosyalar

Koleksiyon

WoS İndeksli Yayınlar Koleksiyonu
Scopus İndeksli Yayınlar Koleksiyonu