Spectroscopic and structural properties of N-(acetamide) morpholinium bromide
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Tarih
2011
Dergi Başlığı
Dergi ISSN
Cilt Başlığı
Yayıncı
Pergamon-Elsevier Science Ltd
Erişim Hakkı
info:eu-repo/semantics/closedAccess
Özet
A new crystal of N-(acetamide) morpholinium (NAM) bromide has been prepared in methanol at room temperature and characterized by single crystal X-ray analysis, elemental analysis, GS-MS, FUR, NMR((1)H, (13)C, DEPTH and HETCOR). The N-(acetamide) morpholinium crystallizes in the orthorhombic crystal system, Pnma with unit cell a = 12.798(9) angstrom, b = 7.222(5) angstrom, c = 9.244(5) angstrom, beta = 90.00, V = 854.4(9) angstrom(3), Z = 4. The X-ray structure determination revealed that there are strong inner and intermolecular hydrogen bonds in the crystal. (C) 2011 Elsevier B.V. All rights reserved.
Açıklama
Anahtar Kelimeler
Morpholine derivative, Spectroscopy, Structure, X-ray, NMR, HETCOR
Kaynak
Spectrochimica Acta Part A-Molecular and Biomolecular Spectroscopy
WoS Q Değeri
Q2
Scopus Q Değeri
Q1
Cilt
81
Sayı
1
