Microwave assisted synthesis of Jeffamine cored PAMAM dendrimers

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dc.authoridErturk, Ali Serol/0000-0001-5352-7939
dc.authoridPARALI, Tezcan/0000-0001-7263-3139
dc.contributor.authorErturk, Ali S.
dc.contributor.authorTulu, Metin
dc.contributor.authorBozdogan, Abdurrezzak E.
dc.contributor.authorParali, Tezcan
dc.date.accessioned2025-01-27T20:52:05Z
dc.date.available2025-01-27T20:52:05Z
dc.date.issued2014
dc.departmentÇanakkale Onsekiz Mart Üniversitesi
dc.description.abstractThis study reports the use of a new microwave assisted amidation method for the synthesis of Jeffamine cored poly (amidoamine) (PAMAM) dendrimers up to fourth generations. Reaction proceeding is monitored by attenuated total reflectance (ATR) without final purification. It was found that current method decreases the aminolysis time, and minimizes the excessive use of reagents and solvents. Synthesized dendrimers were purified by liquid-phase polymer-based retention (LPR) technique and characterized by H-1-NMR, C-13-NMR, EA, GPC and UV-VIS spectroscopy. (C) 2014 Elsevier Ltd. All rights reserved.
dc.description.sponsorshipYildiz Technical University Scientific Research Projects Coordination Department [2011-01-02-KAP04, 2011-01-02-KAP05, 2011-01-02-KAP06, 2012-01-02-DOP05]; EU [2010-1-TR1-LEO05-16728]
dc.description.sponsorshipThis research has been supported by Yildiz Technical University Scientific Research Projects Coordination Department. Project Numbers (2011-01-02-KAP04, 2011-01-02-KAP05, 2011-01-02-KAP06 and 2012-01-02-DOP05) and EU Lifelong Learning Programme (Webgentech Project number: 2010-1-TR1-LEO05-16728).
dc.identifier.doi10.1016/j.eurpolymj.2013.12.018
dc.identifier.endpage226
dc.identifier.issn0014-3057
dc.identifier.issn1873-1945
dc.identifier.scopus2-s2.0-84893187562
dc.identifier.scopusqualityQ1
dc.identifier.startpage218
dc.identifier.urihttps://doi.org/10.1016/j.eurpolymj.2013.12.018
dc.identifier.urihttps://hdl.handle.net/20.500.12428/25654
dc.identifier.volume52
dc.identifier.wosWOS:000332436100021
dc.identifier.wosqualityQ1
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherPergamon-Elsevier Science Ltd
dc.relation.ispartofEuropean Polymer Journal
dc.relation.publicationcategoryinfo:eu-repo/semantics/openAccess
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.snmzKA_WoS_20250125
dc.subjectAmidation
dc.subjectDendrimers
dc.subjectLiquid phase polymer retention (LPR)
dc.subjectMicrowave chemistry (MW)
dc.titleMicrowave assisted synthesis of Jeffamine cored PAMAM dendrimers
dc.typeArticle

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