Synthesis, characterization, electrochemical and surface morphology properties of poly(azomethine-ester)s

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dc.authoridKaya, Ismet/0000-0002-9813-2962
dc.authoridTemizkan Ozdamar, Kevser/0000-0001-7740-3252
dc.contributor.authorTemizkan, Kevser
dc.contributor.authorKaya, İsmet
dc.date.accessioned2025-01-27T20:29:16Z
dc.date.available2025-01-27T20:29:16Z
dc.date.issued2017
dc.departmentÇanakkale Onsekiz Mart Üniversitesi
dc.description.abstractIn this study, poly(azomethine-ester) s (PAEs) were synthesized via elimination reactions of aromatic dihydroxy compounds containing imine bonding with terephthaloyl chloride. The structures of PAEs containing different aliphatic chains and ether bridges were confirmed by FT-IR, H-1, C-13-NMR and UV-Vis measurements. Electrochemical parameters of the synthesized SBs and PAEs were determined by cyclic voltammetry measurements. Thermal properties of the synthesized monomers and polymers were investigated by TG-DTA, DMA and DSC techniques. Molecular mass distributions of PAEs are determined with gel permeation chromatography measurements. Morphological and topographic properties of the SBs and PAEs containing azomethine linkage in the main chain were investigated by SEM and AFM techniques, respectively. Maximum particle sizes on surfaces of polymers were calculated with AFM analyses. Surface modifications of poly(azomethine-ester) s and maximum particle size on their surface were studied with topographic and 3D AFM images and particular size curves.
dc.identifier.doi10.1007/s00289-016-1851-8
dc.identifier.endpage2592
dc.identifier.issn0170-0839
dc.identifier.issn1436-2449
dc.identifier.issue7
dc.identifier.scopus2-s2.0-84994745668
dc.identifier.scopusqualityQ1
dc.identifier.startpage2575
dc.identifier.urihttps://doi.org/10.1007/s00289-016-1851-8
dc.identifier.urihttps://hdl.handle.net/20.500.12428/22889
dc.identifier.volume74
dc.identifier.wosWOS:000403055600009
dc.identifier.wosqualityQ3
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherSpringer
dc.relation.ispartofPolymer Bulletin
dc.relation.publicationcategoryinfo:eu-repo/semantics/openAccess
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.snmzKA_WoS_20250125
dc.subjectPoly(azomethine-ester)
dc.subjectElectrochemical properties
dc.subjectThermal degradation
dc.subjectAFM
dc.subjectSEM
dc.subjectFluorescence properties
dc.titleSynthesis, characterization, electrochemical and surface morphology properties of poly(azomethine-ester)s
dc.typeArticle

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