Spectroscopic Studies and Structure of 4-(3-Benzoylthioureido)benzoic Acid

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dc.authoridUnver, Huseyin/0000-0003-3968-4385
dc.contributor.authorAydin, Fatma
dc.contributor.authorUnver, Huseyin
dc.contributor.authorAykac, Dogan
dc.contributor.authorIskeleli, Nazan Ocak
dc.date.accessioned2025-01-27T21:01:58Z
dc.date.available2025-01-27T21:01:58Z
dc.date.issued2010
dc.departmentÇanakkale Onsekiz Mart Üniversitesi
dc.description.abstract4-(3-Benzoylthioureido)benzoic acid has been synthesized from the reaction of 4-aminobenzoic acid with benzoyl isothiocyanate. The title compound has been characterized by elemental analysis, MS, FT-IR, H-1-NMR, C-13-NMR and UV-Visible techniques. The structure of the compound has also been examined crystallographically. The title compound crystallizes in the triclinic space group P-1 with a = 3.969(1), b = 13.039(1), c = 13.504(1) angstrom, alpha = 96.50(1)degrees, beta = 92.25(1)degrees, gamma = 94.94(1), V = 691.0(1) angstrom(3) and D-x = 1.444 g cm(-3), respectively. The crystal structure has been solved by direct methods and refined by full-matrix least squares and found R (1) = 0.031 and wR (2) = 0.081 for 2909 observed reflections [I > 2 sigma(I)].
dc.description.sponsorshipCanakkale Onsekiz Mart University Grants Commission [2008/35]
dc.description.sponsorshipThe authors thank Canakkale Onsekiz Mart University Grants Commission for a research grant (Project Number: 2008/35).
dc.identifier.doi10.1007/s10870-010-9799-2
dc.identifier.endpage1086
dc.identifier.issn1074-1542
dc.identifier.issn1572-8854
dc.identifier.issue12
dc.identifier.scopus2-s2.0-78650006094
dc.identifier.scopusqualityQ3
dc.identifier.startpage1082
dc.identifier.urihttps://doi.org/10.1007/s10870-010-9799-2
dc.identifier.urihttps://hdl.handle.net/20.500.12428/27245
dc.identifier.volume40
dc.identifier.wosWOS:000284365300008
dc.identifier.wosqualityQ4
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherSpringer/Plenum Publishers
dc.relation.ispartofJournal of Chemical Crystallography
dc.relation.publicationcategoryinfo:eu-repo/semantics/openAccess
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.snmzKA_WoS_20250125
dc.subjectThiourea
dc.subjectBenzoic acid
dc.subjectSpectroscopy
dc.subjectCrystal structure
dc.subjectHydrogen bonds
dc.titleSpectroscopic Studies and Structure of 4-(3-Benzoylthioureido)benzoic Acid
dc.typeArticle

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