Synthesis, Spectral Properties and Structure of New Novel 3,3'-Dibenzoyl-1,1'-(propan-1,3-diyl)-bisthiourea

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dc.authoridUnver, Huseyin/0000-0003-3968-4385
dc.contributor.authorAydin, Fatma
dc.contributor.authorAykac, Dogan
dc.contributor.authorUnver, Huseyin
dc.contributor.authorIskeleli, Nazan Ocak
dc.date.accessioned2025-01-27T20:16:31Z
dc.date.available2025-01-27T20:16:31Z
dc.date.issued2012
dc.departmentÇanakkale Onsekiz Mart Üniversitesi
dc.description.abstractA new 3,3'-dibenzoyl-1,1'-propan-1,3-diyl)bisthiourea was synthesized by using benzoylisothiocyanate with 1,3-diaminopropane in aprotic solvent. The structure was determinated by means of FT-IR, H-1-NMR, C-13-NMR and mass spectroscopic techniques. The crystal structure of 3,3'-dibenzoyl-1,1'-(propan-1,3-diyl)bisthiourea has also been examined by using X-ray crystallographic techniques and found to be crystallized in the monoclinic space group P2 (1) /c with the unit cell parameters: a = 5.968(1) , b = 19.471(2) , c = 16.585(2) , beta = 98.32(1)A degrees, V = 1907.0(4) (3), Dx = 1.395 g cm(-3), and Z = 4 respectively.
dc.description.sponsorshipCanakkale Onsekiz Mart University [BAP-2008-35]
dc.description.sponsorshipThe synthesis section of this study is a part of Dogan AYKAC's Ms Thesis and was supported by Canakkale Onsekiz Mart University Research Fund (Project No: BAP-2008-35).
dc.identifier.doi10.1007/s10870-011-0258-5
dc.identifier.endpage387
dc.identifier.issn1074-1542
dc.identifier.issn1572-8854
dc.identifier.issue4
dc.identifier.scopus2-s2.0-84861344808
dc.identifier.scopusqualityQ3
dc.identifier.startpage381
dc.identifier.urihttps://doi.org/10.1007/s10870-011-0258-5
dc.identifier.urihttps://hdl.handle.net/20.500.12428/21266
dc.identifier.volume42
dc.identifier.wosWOS:000301792600015
dc.identifier.wosqualityQ4
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherSpringer/Plenum Publishers
dc.relation.ispartofJournal of Chemical Crystallography
dc.relation.publicationcategoryinfo:eu-repo/semantics/openAccess
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.snmzKA_WoS_20250125
dc.subjectBisthiourea
dc.subjectCrystal structure determination
dc.subjectSpectroscopic studies
dc.subjectFT-IR
dc.titleSynthesis, Spectral Properties and Structure of New Novel 3,3'-Dibenzoyl-1,1'-(propan-1,3-diyl)-bisthiourea
dc.typeArticle

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