Synthesis, characterization and electrochemical properties of poly (phenoxy-imine)s containing carbazole unit

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dc.authoridKaya, İsmet / 0000-0002-9813-2962
dc.authoridKaraer Yağmur, Hatice / 0000-0002-3728-1825
dc.contributor.authorKaya, İsmet
dc.contributor.authorÇöpür, Sebra
dc.contributor.authorKaraer, Hatice
dc.date.accessioned2025-01-27T20:26:54Z
dc.date.available2025-01-27T20:26:54Z
dc.date.issued2017
dc.departmentÇanakkale Onsekiz Mart Üniversitesi
dc.descriptionThis article is distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution, and reproduction in any medium, provided you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made.
dc.description.abstractSeveral new Schiff base polymers were synthesized via oxidative polymerization method in an aqueous alkaline medium in the presence of NaOCl as an oxidant and were confirmed by FT-IR, H-1-NMR, C-13-NMR and UV-Vis spectroscopic techniques. Furthermore, cyclic voltammetry measurements were carried out and the HOMO-LUMO energy levels and electrochemical band gaps (E-g') were calculated. Additionally, the optical band gaps (E-g) were determined using their UV-Vis spectra of the materials. The morphologic properties of the polymers were investigated by scanning electron microscopy. In addition, the number average molecular weight (M-n), weight average molecular weight (M-w) and polydispersity index values of the polymers were determined by gel permeation chromatography technique. Electrical conductivity measurements of the doped (with iodine) and undoped polymer related to doping time were carried out by four-point probe technique using a Keithley 2400 electrometer. Their thermal behaviors were determined by TG-DTA and DSC measurements. The synthesized compounds were soluble in common solvents such as DMF, THF and DMSO. Photoluminescence properties of the polymers were determined in different concentrations of DMF solvent.
dc.identifier.doi10.1007/s40090-017-0112-5
dc.identifier.endpage343
dc.identifier.issn2228-5547
dc.identifier.issue3
dc.identifier.scopus2-s2.0-85020032767
dc.identifier.scopusqualityN/A
dc.identifier.startpage329
dc.identifier.urihttps://doi.org/10.1007/s40090-017-0112-5
dc.identifier.urihttps://hdl.handle.net/20.500.12428/22489
dc.identifier.volume8
dc.identifier.wosWOS:000411118900009
dc.identifier.wosqualityN/A
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherSpringer Heidelberg
dc.relation.ispartofInternational Journal of Industrial Chemistry
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/openAccess
dc.snmzKA_WoS_20250125
dc.subjectCarbazole
dc.subjectFluorescence
dc.subjectThermal analysis
dc.subjectPoly(phenoxy-imine)
dc.subjectBand gaps
dc.titleSynthesis, characterization and electrochemical properties of poly (phenoxy-imine)s containing carbazole unit
dc.typeArticle

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