Synthesis, spectroscopic studies and crystal structure of (E)-2-(2,4-dihydroxybenzylidene)thiosemicarbazone and (E)-2-[(1H-indol-3-yl)methylene]thiosemicarbazone

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dc.authoridUnver, Huseyin/0000-0003-3968-4385
dc.authoridKiraz, Askin/0000-0002-2350-8291
dc.contributor.authorYıldız, Mustafa
dc.contributor.authorUnver, Huseyin
dc.contributor.authorErdener, Digdem
dc.contributor.authorKiraz, Askin
dc.contributor.authorIskeleli, Nazan Ocak
dc.date.accessioned2025-01-27T20:56:20Z
dc.date.available2025-01-27T20:56:20Z
dc.date.issued2009
dc.departmentÇanakkale Onsekiz Mart Üniversitesi
dc.description.abstractThiosemicarbazone Schiff bases (1 and 2) derived from 2,4-dihydroxybenzaldehyde, indoline-3-carbaldehyde and thiosemicarbazone have been synthesized and their structures were elucidated by elemental analysis. FT-IR, H-1 NMR, C-13 NMR and UV-visible spectroscopic techniques. The structures of compounds 1 and 2 have also been examined cyrstallographically. The title compounds 1 and 2 crystallize in the monoclinic space group C-2/c and triclinic space group P (1) over bar, with unit cell parameters: a = 21.421 (1) and 7.233(1), b = 4.131(1) and 11.166(1), c = 24.942(2) and 13.648(1) angstrom, V = 1856.1(2) and 1019.5(1) angstrom(3), D-x = 1.512 and 1.422 g cm(-3) and Z = 8 and 4, respectively. (C) 2008 Elsevier B.V. All rights reserved.
dc.identifier.doi10.1016/j.molstruc.2008.09.008
dc.identifier.endpage234
dc.identifier.issn0022-2860
dc.identifier.issn1872-8014
dc.identifier.issue1-3
dc.identifier.scopus2-s2.0-58749114732
dc.identifier.scopusqualityQ1
dc.identifier.startpage227
dc.identifier.urihttps://doi.org/10.1016/j.molstruc.2008.09.008
dc.identifier.urihttps://hdl.handle.net/20.500.12428/26374
dc.identifier.volume919
dc.identifier.wosWOS:000263618500036
dc.identifier.wosqualityQ3
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherElsevier
dc.relation.ispartofJournal of Molecular Structure
dc.relation.publicationcategoryinfo:eu-repo/semantics/openAccess
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.snmzKA_WoS_20250125
dc.subjectThiosemicarbazone
dc.subjectCrystal structure
dc.subjectIndoline-3-carbaldehyde
dc.subjectHydrogen bonding
dc.subjectSpectroscopic studies
dc.titleSynthesis, spectroscopic studies and crystal structure of (E)-2-(2,4-dihydroxybenzylidene)thiosemicarbazone and (E)-2-[(1H-indol-3-yl)methylene]thiosemicarbazone
dc.typeArticle

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