Use of cationic p[2-(acryloyloxy)ethyl] trimethylammonium chloride in hydrogel synthesis and adsorption of methyl orange with jeffamine based crosslinker

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dc.authoridOzay, Hava/0000-0002-4184-7801
dc.contributor.authorGungor, Zeynep
dc.contributor.authorOzay, Hava
dc.date.accessioned2025-01-27T20:11:50Z
dc.date.available2025-01-27T20:11:50Z
dc.date.issued2023
dc.departmentÇanakkale Onsekiz Mart Üniversitesi
dc.description.abstractIn this study, a noncommercial polyetheric-structured jeffamine-based crosslinker was used by being synthesized in the synthesis of a hydrogel of a cationic-structured p[2-(acryloyloxy)ethyl] trimethylammonium chloride p(AETAC). The hydrogels containing crosslinkers with five various percentages (0.1, 0.25, 0.75, 1) were synthesized and were aimed to be used as an adsorption material. For the applications, a 1% crosslinked hydrogel (GEL 5) was utilized for the adsorption of a mono-azo chemically structured anionic characterized methyl orange (C14H14N3NaO3S) (MO) colorant. The structure of the jeffamine-based crosslinker was inspired by FT-IR, H-1-NMR, C-13-NMR, and LC-MS analysis, while the hydrogel structure characterization was elucidated by FT-IR spectroscopy. The morphological structure of the hydrogel was examined using scanning electron microscopy (SEM), SEM-EDX, and elemental mapping methods. Concurrently, the mechanical resistance of GEL 5 was tested, and its swelling behavior was examined in different media and pH values. GEL 5, considered decent adsorbent material owing to its structural qualifications, was used in the toxic MO dye adsorption process. In adsorption studies, the maximum qe value of the GEL 5 hydrogel was 547.34 +/- 40.00 mg/g in 1000 mg/L MO dye solution. Furthermore, desorption studies have shown that it has reusability, which is a crucial factor in adsorbent selection.
dc.description.sponsorship100/2000 PhD Scholarship Program
dc.description.sponsorshipThis study is derived from a part of Zeynep Gungor's doctoral thesis. Zeynep Gungor, supported by the 100/2000 PhD Scholarship Program, would like to thank the Turkish Higher Education Institution (YOK) for its contributions.
dc.identifier.doi10.1080/01932691.2022.2129676
dc.identifier.endpage106
dc.identifier.issn0193-2691
dc.identifier.issn1532-2351
dc.identifier.issue1
dc.identifier.scopus2-s2.0-85140046482
dc.identifier.scopusqualityQ2
dc.identifier.startpage91
dc.identifier.urihttps://doi.org/10.1080/01932691.2022.2129676
dc.identifier.urihttps://hdl.handle.net/20.500.12428/20744
dc.identifier.volume45
dc.identifier.wosWOS:000866040200001
dc.identifier.wosqualityQ4
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherTaylor & Francis Inc
dc.relation.ispartofJournal of Dispersion Science and Technology
dc.relation.publicationcategoryinfo:eu-repo/semantics/openAccess
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.snmzKA_WoS_20250125
dc.subjectJeffamine
dc.subjectglycidyl methacrylate
dc.subject2-(acryloyloxy)ethyl trimethylammonium chloride
dc.subjecthydrogel
dc.subjectadsorption
dc.subjectmethyl orange
dc.titleUse of cationic p[2-(acryloyloxy)ethyl] trimethylammonium chloride in hydrogel synthesis and adsorption of methyl orange with jeffamine based crosslinker
dc.typeArticle

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