Synthesis and Characterization and Thermal Decomposition Kinetics of Poly (quinoline)-Copper Composite
[ X ]
Tarih
2018
Dergi Başlığı
Dergi ISSN
Cilt Başlığı
Yayıncı
Erişim Hakkı
info:eu-repo/semantics/openAccess
Özet
In here, chemical oxidative synthesis of a new poly(quinoline)-coppercomposite was given in one-step pathway. To obtain composite, the coppersulphate and 2-amino-8-quinolinol were used as oxidant and monomer,respectively. The oxidation product obtained was characterized by FTIR, UV-Vis,thermogravimetry (TG), photoluminescence (PL), SEM-EDX, TEM analysis and solidstate conductivity measurements. SEM observations exhibited the presence of a plate-like heterogeneousmorphology. Rod like structures was revealed from TEM images. TEM studies also indicated that the coppernanoparticles were almost uniformly distributed on polymer. The thermaldecomposition kinetics of oxidation product were also studied. For this, the differentmethods such as Coats-Redfern, Flynn-Wall-Ozawa, Tang and Kissinger-Akahira-Sunose were used.
Açıklama
Anahtar Kelimeler
Termodinamik, Kimya, Organik, Mühendislik, Kimya
Kaynak
Celal Bayar Üniversitesi Fen Bilimleri Dergisi
WoS Q Değeri
Scopus Q Değeri
Cilt
14
Sayı
2