Synthesis, characterization, photophysical and surface properties of poly(amino naphthalene) and its poly(azomethine) compound

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dc.authorid0000-0002-9813-2962en_US
dc.authorid-en_US
dc.authorid-en_US
dc.authorscopusid56250747600en_US
dc.authorscopusid57664822000en_US
dc.authorscopusid57337059300en_US
dc.authorwosidABD-2324-2020en_US
dc.authorwosid-en_US
dc.authorwosid-en_US
dc.contributor.authorKaya, İsmet
dc.contributor.authorAkyüz, Burçin
dc.contributor.authorÖzel, Şahin
dc.date.accessioned2023-08-01T06:31:43Z
dc.date.available2023-08-01T06:31:43Z
dc.date.issued2023en_US
dc.departmentFakülteler, Fen Fakültesi, Kimya Bölümü
dc.description.abstractIn this study, 8-((4-hydroxybenzylidene)amino)naphthalene-2-ol (ANAPSB) compound was synthesized from condensation reaction of 8-amino-2-naphthol (ANAP) with 4-hydroxybenzaldehyde and then ANAPSB and 8-amino-2-naphthol were polymerized via oxidative polycondensation alkaline medium by H2O2 (35% aqueous solution) as oxidant at 70°C 14 h. The structures of compounds were confirmed by UV–Vis, 1H-13C-NMR and FT-IR measurements. The surface morphologies of PANAP and PANAPSB were examined with SEM analyses. The electrochemical properties of 8-amino-2-naphthol, poly(8-amino-2-naphthol) (PANAP), ANAPSB and poly(8-((4-hydroxybenzylidene)amino)naphthalene-2-ol) (PANAPSB) were determined by cyclic voltammetry technique. The thermal properties of compounds were found by TG-DTA analysis. The glass transition temperatures (Tg) of PANAP and PANAPSB were determined from DSC measurements. The Tg values of PANAP and PANAPSB were found to be 159 and 150°C, respectively. The Mn, Mw, Mp, Mz and PDI values of the PANAP and PANAPSB were calculated from gel permeation chromatography measurements. The optical and fluorescence properties of the compounds were determined by UV–Vis and fluorescence measurements, respectively. The optical band gap values of ANAP, PANAP, ANAPSB and PANAPSB were calculated as 3.12, 1.61, 2.79 and 1.57 eV, respectively.en_US
dc.identifier.citationİsmet, Kaya, Akyüz, B., & Özel, Ş. (2023). Synthesis, characterization, photophysical and surface properties of poly(amino naphthalene) and its poly(azomethine) compound. Journal of Applied Polymer Science, 140(27). https://doi.org/10.1002/app.54021en_US
dc.identifier.doi10.1002/app.54021
dc.identifier.issn0021-8995
dc.identifier.issn1097-4628
dc.identifier.issue27en_US
dc.identifier.scopus2-s2.0-85157973797
dc.identifier.urihttps://doi.org/10.1002/app.54021
dc.identifier.urihttps://hdl.handle.net/20.500.12428/4466
dc.identifier.volume140en_US
dc.identifier.wosWOS:000980674000001
dc.identifier.wosqualityQ2
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.institutionauthorKaya, İsmet
dc.institutionauthorAkyüz, Burçin
dc.institutionauthorÖzel, Şahin
dc.language.isoen
dc.publisherJohn Wiley and Sons Incen_US
dc.relation.ispartofJournal of Applied Polymer Scienceen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.rightsAttribution 3.0 United States*
dc.rights.urihttp://creativecommons.org/licenses/by/3.0/us/*
dc.subjectFluorescence propertyen_US
dc.subjectOxidative polymerizationen_US
dc.subjectPoly(azomethine)en_US
dc.subjectSchiff baseen_US
dc.titleSynthesis, characterization, photophysical and surface properties of poly(amino naphthalene) and its poly(azomethine) compound
dc.typeArticle

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