Spectroscopic Studies and Crystal Structure of (Z)-6-[(2-hydroxyphenylamino)methylene]-2-methoxycyclohexa-2,4-dienone

dc.authoridUnver, Huseyin/0000-0003-3968-4385
dc.authoridKiraz, Askin/0000-0002-2350-8291
dc.contributor.authorUnver, Huseyin
dc.contributor.authorYıldız, Mustafa
dc.contributor.authorKiraz, Askin
dc.contributor.authorOzgen, Ozen
dc.date.accessioned2025-01-27T20:56:23Z
dc.date.available2025-01-27T20:56:23Z
dc.date.issued2009
dc.departmentÇanakkale Onsekiz Mart Üniversitesi
dc.description.abstractThe Schiff base (Z)-6-[(2-hydroxyphenylamino) methylene]-2-methoxycyclohexa-2,4-dienone has been synthesized from the reaction of 2-aminophenol with 2-hydroxy-3-methoxybenzaldehyde. The title compound has been characterized by elemental analysis, FT-IR, H-1-NMR, C-13-NMR and UV-Visible techniques. The structure of the title compound also was determined crystallographically. The crystal structure has been solved by direct methods and refined by full-matrix least squares. The title compound crystallize in the monoclinic space group P2(1)/c with a = 10.438(1), b = 8.851(1), c = 12.746(1) angstrom, beta = 95.72(1)degrees, V = 1171.7(2) angstrom(3), D-x = 1.379 g cm(-3), respectively (R1 = 0.0522 and wR2 = 0.126 for 1442 reflections [I > 2 sigma(1)]).
dc.identifier.doi10.1007/s10870-008-9412-0
dc.identifier.endpage23
dc.identifier.issn1074-1542
dc.identifier.issn1572-8854
dc.identifier.issue1
dc.identifier.scopus2-s2.0-62549154075
dc.identifier.scopusqualityQ3
dc.identifier.startpage17
dc.identifier.urihttps://doi.org/10.1007/s10870-008-9412-0
dc.identifier.urihttps://hdl.handle.net/20.500.12428/26388
dc.identifier.volume39
dc.identifier.wosWOS:000261957400004
dc.identifier.wosqualityQ4
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherSpringer/Plenum Publishers
dc.relation.ispartofJournal of Chemical Crystallography
dc.relation.publicationcategoryinfo:eu-repo/semantics/openAccess
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.snmzKA_WoS_20250125
dc.subjectSchiff base
dc.subjectSpectroscopy
dc.subjectCrystal structure
dc.subjectO-Vanillin
dc.subjectTautomerisim
dc.titleSpectroscopic Studies and Crystal Structure of (Z)-6-[(2-hydroxyphenylamino)methylene]-2-methoxycyclohexa-2,4-dienone
dc.typeArticle

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