Spectroscopic studies, antimicrobial activities, and crystal structure of N-[2-hydroxy-1-naphthylidene]3,5-bis(trifluoromethyl)aniline

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dc.authoridUnver, Huseyin/0000-0003-3968-4385
dc.authoridDulger, Basaran/0000-0002-3184-2652
dc.authoridKiraz, Askin/0000-0002-2350-8291
dc.contributor.authorÜnver, Hüseyin
dc.contributor.authorYıldız, Mustafa
dc.contributor.authorKiraz, Aşkın
dc.contributor.authorİskeleli, Nazan Ocak
dc.contributor.authorErdönmez, Ahmet
dc.contributor.authorDülger, Başaran
dc.contributor.authorDurlu, Tahsin Nuri
dc.date.accessioned2025-01-27T20:56:23Z
dc.date.available2025-01-27T20:56:23Z
dc.date.issued2006
dc.departmentÇanakkale Onsekiz Mart Üniversitesi
dc.description.abstractA new Schiff base compound has been synthesized by the reaction of 2-hydroxy-1-naphthaldehyde with 3,5-bis(trifluoromethyl)aniline.The title compound was characterized by elemental analysis, IR, H-1 NMR, C-13 NMR, and UV-Visible techniques.Its UV-Vis spectra was examined in polar and nonpolar solvents and in acidic and basic media. The crystal structure of the compound showed the OH group to be ortho to the imine group. It crystallizes in the monoclinic space group P2(1) with a = 11.328(2), b = 6.125(1), c = 11.937(2) angstrom, V = 825.1(2) angstrom(3), D (x) = 1.543 g cm(-3) and Z = 2. An intramolecular O1- H center dot center dot center dot N1 [2.558(7) angstrom] hydrogen bond stabilizes the molecule. The compound has also been characterized by its antimicrobial activities. The ligand has been screened in vitro against the organisms Escherichia coli ATCC 11230, Staphylococcus aureus ATCC 6538, Klebsiella pneumoniae UC57, Micrococcus luteus La 2971, Proteus vulgaris ATCC 8427, Pseudomonas aeruginosa ATCC 27853, Mycobacterium smegmatis CCM 2067, Bacillus cereus ATCC 7064, and Listeria monocytogenes ATCC 15313, the yeast cultures Candida albicans ATCC 10231, Kluyveromyces fragilis NRRL 2415, Rhodotorula rubra DSM 70403, Debaryomyces hansenii DSM 70238, and Hanseniaspora guilliermondii DSM 3432.
dc.identifier.doi10.1007/s10870-005-9053-5
dc.identifier.endpage237
dc.identifier.issn1074-1542
dc.identifier.issn1572-8854
dc.identifier.issue3
dc.identifier.scopus2-s2.0-33746898252
dc.identifier.scopusqualityQ3
dc.identifier.startpage229
dc.identifier.urihttps://doi.org/10.1007/s10870-005-9053-5
dc.identifier.urihttps://hdl.handle.net/20.500.12428/26387
dc.identifier.volume36
dc.identifier.wosWOS:000239591000012
dc.identifier.wosqualityQ4
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherSpringer/Plenum Publishers
dc.relation.ispartofJournal of Chemical Crystallography
dc.relation.publicationcategoryinfo:eu-repo/semantics/openAccess
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.snmzKA_WoS_20250125
dc.subjectSchiff base
dc.subjectspectroscopic studies
dc.subjectcrystal structure
dc.subjecttautomerism
dc.titleSpectroscopic studies, antimicrobial activities, and crystal structure of N-[2-hydroxy-1-naphthylidene]3,5-bis(trifluoromethyl)aniline
dc.typeArticle

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