Oxidative synthesis of a novel polyphenol having pendant Schiff base group: Synthesis, characterization, non-isothermal decomposition kinetics

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dc.authoridKaya, İsmet / 0000-0002-9813-2962
dc.authoridDoğan, Fatih / 0000-0002-3088-886X / 0000-0001-5844-8893
dc.contributor.authorDilek, Deniz
dc.contributor.authorDoğan, Fatih
dc.contributor.authorBilici, Ali
dc.contributor.authorKaya, İsmet
dc.date.accessioned2025-01-27T21:01:51Z
dc.date.available2025-01-27T21:01:51Z
dc.date.issued2011
dc.departmentÇanakkale Onsekiz Mart Üniversitesi
dc.description.abstractIn here, the facile synthesis and thermal characterization of a novel polyphenol containing Schiff base pendant group, poly(4-{[(4-hydroxyphenyl)imino]methyl}benzene-1,2,3-triol) [PHPIMB], are reported. UV-vis, FT-IR,H-1 NMR, C-13 NMR, GPC, TG/DTG-DTA, CV (cyclic voltammetry) and solid state conductivity measurements were utilized to characterize the obtained monomer and polymer. The spectral analyses results showed that PHPIMB was composed of polyphenol main chains containing Schiff base pendant side groups. Thermal properties of the polymer were investigated by thermogravimetric analyses under a nitrogen atmosphere. Five methods were used to study the thermal decomposition of PHPIMB at different heating rate and the results obtained by using all the kinetic methods were compared with each other. The thermal decomposition of PHPIMB was found to be a simple process composed of three stages. These investigated methods were those of Flynn-Wall-Ozawa (FWO), Tang, Kissinger-Akahira-Sunose (KAS), Friedman and Kissinger methods. (C) 2011 Elsevier B.V. All rights reserved.
dc.description.sponsorshipCanakkale Onsekiz Mart University [2010/119]
dc.description.sponsorshipDr. Fatih Doan thanks to Canakkale Onsekiz Mart University Research Fund for support with the project (COMU Project No: 2010/119)
dc.identifier.doi10.1016/j.tca.2011.02.009
dc.identifier.endpage81
dc.identifier.issn0040-6031
dc.identifier.issn1872-762X
dc.identifier.issue1-2
dc.identifier.scopus2-s2.0-79953865787
dc.identifier.scopusqualityQ1
dc.identifier.startpage72
dc.identifier.urihttps://doi.org/10.1016/j.tca.2011.02.009
dc.identifier.urihttps://hdl.handle.net/20.500.12428/27210
dc.identifier.volume518
dc.identifier.wosWOS:000290187400010
dc.identifier.wosqualityQ3
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherElsevier
dc.relation.ispartofThermochimica Acta
dc.relation.publicationcategoryinfo:eu-repo/semantics/openAccess
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.snmzKA_WoS_20250125
dc.subjectOxidative polymerization
dc.subjectThermal analysis
dc.subjectNon-isothermal decomposition kinetics
dc.titleOxidative synthesis of a novel polyphenol having pendant Schiff base group: Synthesis, characterization, non-isothermal decomposition kinetics
dc.typeArticle

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