Preparation and characterization of monodisperse, mesoporous natural poly(tannic acid)-silica nanoparticle composites with antioxidant properties
| dc.authorid | Sağbaş Suner, Selin / 0000-0002-3524-0675 | |
| dc.authorid | Şahiner, Nurettin / 0000-0003-0120-530X | |
| dc.contributor.author | Şahiner, Nurettin | |
| dc.contributor.author | Sağbaş, Selin | |
| dc.contributor.author | Aktaş, Nahit | |
| dc.date.accessioned | 2025-01-27T20:58:03Z | |
| dc.date.available | 2025-01-27T20:58:03Z | |
| dc.date.issued | 2016 | |
| dc.department | Çanakkale Onsekiz Mart Üniversitesi | |
| dc.description.abstract | Mesoporous poly(Tannic Acid)-Silica nanoparticle composites (p(TA)-Si NPs) were prepared via one pot reaction. At various TA amounts in feed, 50,100, 250, 500, 1000 mg at different reaction times, 2, 4, 8,12, 24 h in the presence of TEOS and epoxy crosslinker, trimethylolpropane triglycidyl ether (TMPGDE), NPs composites were readily prepared. The prepared p(TA)-Si NPs by using 1000 mg TA at 12 h reaction time at room temperature as p(TA)1000-Si NPs provided the highest yield (similar to 48%). The particle size, monodispersity, specific surface area, porosity, and the gravimetric yields are greatly depended on initial TA concentration and reaction time. The particles sizes were found as 237-445 nm depending on TA content and reaction time. The highest surface area was measured as 872 m(2)/g for p(TA)1000-Si NPs for 2 h reaction time. The thermal stability of p(TA)-Si NPs decreased as TA content is increased. Interestingly, p(TA)1000-Si NPs are found effective antioxidant materials. (C) 2016 Elsevier Inc. All rights reserved. | |
| dc.description.sponsorship | Scientific and Technological Research Council of Turkey [113Z238] | |
| dc.description.sponsorship | This work is supported by The Scientific and Technological Research Council of Turkey (113Z238). | |
| dc.identifier.doi | 10.1016/j.micromeso.2016.02.012 | |
| dc.identifier.endpage | 324 | |
| dc.identifier.issn | 1387-1811 | |
| dc.identifier.issn | 1873-3093 | |
| dc.identifier.scopus | 2-s2.0-84960847209 | |
| dc.identifier.scopusquality | Q1 | |
| dc.identifier.startpage | 316 | |
| dc.identifier.uri | https://doi.org/10.1016/j.micromeso.2016.02.012 | |
| dc.identifier.uri | https://hdl.handle.net/20.500.12428/26594 | |
| dc.identifier.volume | 226 | |
| dc.identifier.wos | WOS:000373419400038 | |
| dc.identifier.wosquality | Q1 | |
| dc.indekslendigikaynak | Web of Science | |
| dc.indekslendigikaynak | Scopus | |
| dc.language.iso | en | |
| dc.publisher | Elsevier Science Bv | |
| dc.relation.ispartof | Microporous and Mesoporous Materials | |
| dc.relation.publicationcategory | Makale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı | |
| dc.rights | info:eu-repo/semantics/closedAccess | |
| dc.snmz | KA_WoS_20250125 | |
| dc.subject | Tannic acid/silica | |
| dc.subject | Composite mesoporous nanoparticles | |
| dc.subject | Antioxidant natural polymer composites | |
| dc.subject | Microgel/nanogel composite | |
| dc.title | Preparation and characterization of monodisperse, mesoporous natural poly(tannic acid)-silica nanoparticle composites with antioxidant properties | |
| dc.type | Article |
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