Spectroscopic studies, antimicrobial activities and crystal structures of N-(2-hydroxy-3-methoxybenzalidene) 1-aminonaphthalene

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dc.authoridUnver, Huseyin/0000-0003-3968-4385
dc.authoridDulger, Basaran/0000-0002-3184-2652
dc.contributor.authorÜnver, H
dc.contributor.authorYildiz, M
dc.contributor.authorDülger, B
dc.contributor.authorÖzgen, Ö
dc.contributor.authorKendi, E
dc.contributor.authorDurlu, TN
dc.date.accessioned2025-01-27T20:56:24Z
dc.date.available2025-01-27T20:56:24Z
dc.date.issued2005
dc.departmentÇanakkale Onsekiz Mart Üniversitesi
dc.description.abstractSchiff base N-(2-hydroxy-3-methoxybenzalidene)1-aminonaphthalene has been synthesized from the reaction of 2-hydroxy-3-methoxybenzaldehyde with 1-aminonaphthalene. The compound were characterized by elemental analysis, FT-IR, H-1 NMR, C-13 NMR and UV-visible techniques. The UV-visible spectra of the Schiff base were studied in polar and nonpolar solvents in acidic and basic media. The structure of the compound has been examined cyrstallographically. There are two independent molecules in the asymmetric unit. It crystallizes in the monoclinic space group P2(l)/c, with unit cell parameters: a=14,602(2), b=5,800(1), c= 16,899(1) Angstrom, V= 1394.4(2) Angstrom(3) D-x=1.321 g cm(-3) and Z = 4. The crystal structure was solved by direct methods and refined by full-matrix least squares to a find R = 0.041 of for 1179 observed reflections. The title compound's antimicrobial activities also have been studied. The antimicrobial activities of the ligand has been screened in vitro against the organisms Escherichia coli ATCC 11230, Staphylococcus aureus ATCC 6538, Klebsiella pneumoniae UC57, Micrococcus luteus La 2971, Proteus vulgaris ATCC 8427, Pseudomonas aeruginosa ATCC 27853, Mycobacterium smegmatis CCM 2067, Bacillus cereus ATCC 7064 and Listeria monocytogenes ATCC 15313, the yeast cultures Candida albicans ATCC 1023 1, Kluyveromyces fragilis NRRL 2415, Rhodotorula rubra DSM 70403, Debaryomyces hansenii DSM 70238 and Hanseniaspora guilliemodii DSM 3432. (C) 2004 Elsevier B.V. All rights reserved.
dc.identifier.doi10.1016/j.molstruc.2004.10.030
dc.identifier.endpage164
dc.identifier.issn0022-2860
dc.identifier.issn1872-8014
dc.identifier.issue2-3
dc.identifier.scopus2-s2.0-12844278911
dc.identifier.scopusqualityQ1
dc.identifier.startpage159
dc.identifier.urihttps://doi.org/10.1016/j.molstruc.2004.10.030
dc.identifier.urihttps://hdl.handle.net/20.500.12428/26391
dc.identifier.volume737
dc.identifier.wosWOS:000227082800012
dc.identifier.wosqualityQ3
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherElsevier
dc.relation.ispartofJournal of Molecular Structure
dc.relation.publicationcategoryinfo:eu-repo/semantics/openAccess
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.snmzKA_WoS_20250125
dc.subjectspectroscopic studies
dc.subjectligand
dc.subjectenol-imine form
dc.subjecttautomerism
dc.subjectantimicrobial activities
dc.titleSpectroscopic studies, antimicrobial activities and crystal structures of N-(2-hydroxy-3-methoxybenzalidene) 1-aminonaphthalene
dc.typeArticle

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