Spectroscopic studies and crystal structure of (E)-N?-(2-hydroxy-3-methoxybenzylidene)isonicotinohydrazide
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Tarih
2013
Yazarlar
Dergi Başlığı
Dergi ISSN
Cilt Başlığı
Yayıncı
Pleiades Publishing Inc
Erişim Hakkı
info:eu-repo/semantics/closedAccess
Özet
The structure of compound has also been examined cyrstallographically. It crystallizes in the monoclinic space group P2(1)/c with a = 7.673(1), b = 16.251(2), c = 10.874(1) , beta = 110.42(1)A degrees, V = 1270.7(3) (3), D (x) = 1.418 g cm(-3), R (1) = 0.0349 and wR (2) = 0.0935 [I > 2 sigma(I)], respectively. The title compound has been synthesized from the reaction of isonicotinohydrazide with 2-hydroxy-3-methoxybenzaldehyde. It has been characterized by using elemental analysis, MS, IR, H-1 NMR, C-13 NMR and UV-Visible spectroscopic techniques.
Açıklama
Anahtar Kelimeler
Schiff-Bases, Antimycobacterial Activity, Solid-State, Tautomerism, Complexes, Photochromism, Mesomorphism, Adducts, Copper, Nickel
Kaynak
Crystallography Reports
WoS Q Değeri
Q4
Scopus Q Değeri
Q4
Cilt
58
Sayı
1