Characterization of Plasma-Polymerized Thiophene Thin Films and Nanoparticles Synthesized by a Double-Discharge Technique

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dc.authoridGoktas, Hilal/0000-0003-2897-0036
dc.contributor.authorGoktas, Hilal
dc.contributor.authorInce, Fatma Gul
dc.date.accessioned2025-01-27T20:59:38Z
dc.date.available2025-01-27T20:59:38Z
dc.date.issued2009
dc.departmentÇanakkale Onsekiz Mart Üniversitesi
dc.description.abstractPTH nanoparticles and thin films were synthesized via a plasma polymerization technique using a double-discharge system. This system has a fast filamentary discharge formed from the superposition of an ordinary low-pressure dc glow discharge and a high-current pulsed one. The samples were characterized by SEM, TEM, XPS, UV-vis and FT-IR spectroscopy. We found that superposing two discharges allows to control the morphology of the films. In the high-temperature region, smooth and uniform thin films were produced, whereas gas-phase polymerization resulted in films with grains of irregular shape. However, the films produced in the gas-phase region exhibited highly thiophenic structures and could be dispersed in DCM, giving nanoparticles of 30 to 50 nm diameter.
dc.identifier.doi10.1002/ppap.200800077
dc.identifier.endpage131
dc.identifier.issn1612-8850
dc.identifier.issue2
dc.identifier.scopus2-s2.0-67349169826
dc.identifier.scopusqualityQ1
dc.identifier.startpage126
dc.identifier.urihttps://doi.org/10.1002/ppap.200800077
dc.identifier.urihttps://hdl.handle.net/20.500.12428/26762
dc.identifier.volume6
dc.identifier.wosWOS:000263636200005
dc.identifier.wosqualityQ1
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherWiley-V C H Verlag Gmbh
dc.relation.ispartofPlasma Processes and Polymers
dc.relation.publicationcategoryinfo:eu-repo/semantics/openAccess
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.snmzKA_WoS_20250125
dc.subjectDC discharges
dc.subjectfilamentary discharges
dc.subjectnanostructures
dc.subjectpolymerization
dc.subjectthin films
dc.titleCharacterization of Plasma-Polymerized Thiophene Thin Films and Nanoparticles Synthesized by a Double-Discharge Technique
dc.typeArticle

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