Spectroscopic Studies and Crystal Structure of 4-(2-Hydroxy-3-Methoxybenzylideneamino)-N-(5-Methylisoxazol-3-yl) Benzenesulfonamide
| dc.authorid | Unver, Huseyin/0000-0003-3968-4385 | |
| dc.contributor.author | Yıldız, Mustafa | |
| dc.contributor.author | Unver, Hueseyin | |
| dc.contributor.author | Erdener, Digdem | |
| dc.contributor.author | Iskeleli, Nazan Ocak | |
| dc.date.accessioned | 2025-01-27T20:56:24Z | |
| dc.date.available | 2025-01-27T20:56:24Z | |
| dc.date.issued | 2010 | |
| dc.department | Çanakkale Onsekiz Mart Üniversitesi | |
| dc.description.abstract | Schiff base 4-[(2-hydroxy-3-methoxybenzylideneamino)-N-(5-methylisoxazol-3-yl)benzene-sulfonamidehas been synthesized from the reaction of 4-amino-N-(5-methylisoxazol-3-yl)benzenesulfonamide(sulfamethoxazole) with 2-hydroxy-3-methoxybenzaldehyde. It has been characterized by elemental analysis, MS, IR, H-1 NMR, C-13 NMR, HET-COR and UV-Visible techniques. The structure of it also has been examined crystallographically. For the compound exist as dominant form of enol-imines in both the solid state and the solutions. It crystallizes in the monoclinic space group P2(1)/c with a = 8.2694(7), b = 8.3453( 5), c = 26.260( 2) angstrom, beta = 97.142(7)degrees, V = 1798.1(2) angstrom(3) , D-x = 1.431 g cm(-3), R-1 = 0.0529 and wR(2) = 0.1370 [ I > 2 sigma(I)], respectively. | |
| dc.identifier.doi | 10.1007/s10870-010-9723-9 | |
| dc.identifier.endpage | 695 | |
| dc.identifier.issn | 1074-1542 | |
| dc.identifier.issn | 1572-8854 | |
| dc.identifier.issue | 8 | |
| dc.identifier.startpage | 691 | |
| dc.identifier.uri | https://doi.org/10.1007/s10870-010-9723-9 | |
| dc.identifier.uri | https://hdl.handle.net/20.500.12428/26393 | |
| dc.identifier.volume | 40 | |
| dc.identifier.wos | WOS:000279197600012 | |
| dc.identifier.wosquality | Q4 | |
| dc.indekslendigikaynak | Web of Science | |
| dc.language.iso | en | |
| dc.publisher | Springer/Plenum Publishers | |
| dc.relation.ispartof | Journal of Chemical Crystallography | |
| dc.relation.publicationcategory | info:eu-repo/semantics/openAccess | |
| dc.rights | info:eu-repo/semantics/closedAccess | |
| dc.snmz | KA_WoS_20250125 | |
| dc.subject | Schiff base | |
| dc.subject | Spectroscopy | |
| dc.subject | Crystal structure | |
| dc.subject | Tautomerisim | |
| dc.subject | Hydrogen bonds | |
| dc.title | Spectroscopic Studies and Crystal Structure of 4-(2-Hydroxy-3-Methoxybenzylideneamino)-N-(5-Methylisoxazol-3-yl) Benzenesulfonamide | |
| dc.type | Article |
