Synthesis, Spectroscopic Studies and Structure of 2-[(Benzo[d]thiazol-2-ylamino)methyl]phenol

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dc.authoridUnver, Huseyin/0000-0003-3968-4385
dc.authoridOzay, Hava/0000-0002-4184-7801
dc.contributor.authorYıldız, Mustafa
dc.contributor.authorOzay, Hava
dc.contributor.authorUnver, Huseyin
dc.contributor.authorIskeleli, Nazan Ocak
dc.contributor.authorZengin, D. Mehmet
dc.contributor.authorDurlu, Tahsin Nuri
dc.date.accessioned2025-01-27T20:56:20Z
dc.date.available2025-01-27T20:56:20Z
dc.date.issued2010
dc.departmentÇanakkale Onsekiz Mart Üniversitesi
dc.description.abstractSchiff base (E)-2-[(benzo[d]thiazol-2-ylimino)methyl]phenol (1) has been synthesized from the reaction of 2-hydroxy-benzaldehyde with 2-aminobenzothiazole The 2-[(benzo[d]thiazol-2-ylamino)methyl]phenol (2) was prepared reduction of the Schiff base 1 with sodium borohydride The compounds 1 and 2 have been characterized by elemental analysis, FT-IR, H-1-NMR, C-13-NMR and UV-visible spectroscopic techniques The structure of the compound 2 has also been examined crystallographically The compound 2 crystallizes in the monoclinic space group P2/c The unit cell parameters were found as a = 10 017(1), b = 11 725(1), c = 10 341(1) angstrom, V = 1208 1(1) A(3), D-x = 1 409 g cm(-3) and Z = 4 The crystal structure was solved by direct methods and refined by the full-matrix least squares method and found as R-1 = 0 0308 and wR(2) = 0 0818 for 2032 for the observed reflections [1 > 2 sigma(1)]
dc.identifier.doi10.1007/s10870.010.9761.3
dc.identifier.endpage913
dc.identifier.issn1074-1542
dc.identifier.issn1572-8854
dc.identifier.issue11
dc.identifier.startpage909
dc.identifier.urihttps://doi.org/10.1007/s10870.010.9761.3
dc.identifier.urihttps://hdl.handle.net/20.500.12428/26375
dc.identifier.volume40
dc.identifier.wosWOS:000284078600003
dc.identifier.wosqualityQ4
dc.indekslendigikaynakWeb of Science
dc.language.isoen
dc.publisherSpringer/Plenum Publishers
dc.relation.ispartofJournal of Chemical Crystallography
dc.relation.publicationcategoryinfo:eu-repo/semantics/openAccess
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.snmzKA_WoS_20250125
dc.subjectCrystal structure
dc.subjectSpectroscopic studies
dc.subjectFT-IR
dc.subjectUV-visible
dc.subjectNMR
dc.titleSynthesis, Spectroscopic Studies and Structure of 2-[(Benzo[d]thiazol-2-ylamino)methyl]phenol
dc.typeArticle

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