Aydin, FatmaUnver, HuseyinAykac, DoganIskeleli, Nazan Ocak2025-01-272025-01-2720101074-15421572-8854https://doi.org/10.1007/s10870-010-9799-2https://hdl.handle.net/20.500.12428/272454-(3-Benzoylthioureido)benzoic acid has been synthesized from the reaction of 4-aminobenzoic acid with benzoyl isothiocyanate. The title compound has been characterized by elemental analysis, MS, FT-IR, H-1-NMR, C-13-NMR and UV-Visible techniques. The structure of the compound has also been examined crystallographically. The title compound crystallizes in the triclinic space group P-1 with a = 3.969(1), b = 13.039(1), c = 13.504(1) angstrom, alpha = 96.50(1)degrees, beta = 92.25(1)degrees, gamma = 94.94(1), V = 691.0(1) angstrom(3) and D-x = 1.444 g cm(-3), respectively. The crystal structure has been solved by direct methods and refined by full-matrix least squares and found R (1) = 0.031 and wR (2) = 0.081 for 2909 observed reflections [I > 2 sigma(I)].eninfo:eu-repo/semantics/closedAccessThioureaBenzoic acidSpectroscopyCrystal structureHydrogen bondsArticle40121082108610.1007/s10870-010-9799-2Q4WOS:0002843653000082-s2.0-78650006094Q3