Yıldız, MustafaUnver, HuseyinErdener, DigdemKiraz, AskinIskeleli, Nazan Ocak2025-01-272025-01-2720090022-28601872-8014https://doi.org/10.1016/j.molstruc.2008.09.008https://hdl.handle.net/20.500.12428/26374Thiosemicarbazone Schiff bases (1 and 2) derived from 2,4-dihydroxybenzaldehyde, indoline-3-carbaldehyde and thiosemicarbazone have been synthesized and their structures were elucidated by elemental analysis. FT-IR, H-1 NMR, C-13 NMR and UV-visible spectroscopic techniques. The structures of compounds 1 and 2 have also been examined cyrstallographically. The title compounds 1 and 2 crystallize in the monoclinic space group C-2/c and triclinic space group P (1) over bar, with unit cell parameters: a = 21.421 (1) and 7.233(1), b = 4.131(1) and 11.166(1), c = 24.942(2) and 13.648(1) angstrom, V = 1856.1(2) and 1019.5(1) angstrom(3), D-x = 1.512 and 1.422 g cm(-3) and Z = 8 and 4, respectively. (C) 2008 Elsevier B.V. All rights reserved.eninfo:eu-repo/semantics/closedAccessThiosemicarbazoneCrystal structureIndoline-3-carbaldehydeHydrogen bondingSpectroscopic studiesArticle9191-322723410.1016/j.molstruc.2008.09.008Q3WOS:0002636185000362-s2.0-58749114732Q1